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Influence of B2O3 addition on the properties of TiO2 thick film at various annealing temperatures for hydrogen sensing


Citation

Mohd Chachuli, Siti Amaniah and Hamidon, Mohd Nizar and Ertugrul, Mehmet and Mamat @ Mat Nazir, Md. Shuhazlly and Jaafar, Haslina and Azis, Norhafiz (2020) Influence of B2O3 addition on the properties of TiO2 thick film at various annealing temperatures for hydrogen sensing. Journal of Electronic Materials, 49. 3340 - 3349. ISSN 0361-5235; ESSN: 1543-186X

Abstract

To increase the adhesion of thick film on a substrate, boron oxide (B2O3) was added to titanium dioxide (TiO2), and the change in the morphology, crystallinity and band gap of TiO2 thick film was investigated. TiO2 and TiO2-B2O3 pastes were prepared and deposited on the microscopic glass using screen-printing technique and then annealed under air at different temperatures of 400°C, 450°C and 500°C for 30 min. The morphology, elemental composition, structure and absorption of the thick films were characterized using FESEM, EDX, XRD and UV–visible spectroscopy. The TiO2 and TiO2-B2O3 thick films were fabricated as gas sensors and exposed to 100–1000 ppm of hydrogen at an operating temperature of 300°C. The results revealed that the addition of B2O3 increased the crystallinity of anatase phases and rutile phases in TiO2 as annealing temperature increased. The TiO2-B2O3(T500) gas sensor exhibited the highest response to various concentrations of hydrogen (100–1000 ppm) at an operating temperature of 300°C.


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Additional Metadata

Item Type: Article
Divisions: Faculty of Engineering
Faculty of Science
Institute of Advanced Technology
DOI Number: https://doi.org/10.1007/s11664-020-08059-0
Publisher: Springer
Keywords: TiO2-B2O3; Screen printing; Thick film; Hydrogen gas sensor; Adhesion
Depositing User: Ms. Nuraida Ibrahim
Date Deposited: 17 Sep 2021 22:14
Last Modified: 17 Sep 2021 22:14
Altmetrics: http://www.altmetric.com/details.php?domain=psasir.upm.edu.my&doi=10.1007/s11664-020-08059-0
URI: http://psasir.upm.edu.my/id/eprint/89353
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