UPM Institutional Repository

Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method


Citation

Hashim, Norhayati and Muda, Zuhailimuna and Mohd Sharif, Sharifah Norain and Md Isa, Illyas and Mohd Ali, Noorshida and Ghazuli, Mohammad Rafaei and Hussein, Mohd Zobir (2016) Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method. Materials Research Innovations, 21 (6). 396 - 400. ISSN 1433-075X

Abstract

The intercalation of chloroacetic acid (CAA) into the interlayer gallery of zinc layered hydroxide has been achieved via a facile direct reaction method. The nanohybrid synthesised, zinc layered hydroxide-chloroacetate was characterised using Powder X-ray diffraction patterns (PXRD), which demonstrated the progressive evolution of the nanohybrid structure, as the CAA molarity were increased from 0.05 to 0.3 M. Sharp and symmetrical peaks of 0.3 M CAA were observed in the PXRD pattern. The emergence of intercalation peak, with basal spacing of 14.3 Å signifying the success intercalation of chloroacetate anions into the interlayer space of the host. The intercalation was also validated by FTIR spectroscopy and CHNS elemental analyser. The increased thermal stability of zinc layered hydroxide-chloroacetate nanohybrid was confirmed by thermogravimetric analysis.


Download File

[img] Text
Preparation of zinc layered .pdf
Download (45kB)

Additional Metadata

Item Type: Article
Divisions: Faculty of Science
Institute of Advanced Technology
DOI Number: https://doi.org/10.1080/14328917.2016.1265248
Publisher: Taylor & Francis
Keywords: Nanohybrid; Chloroacetate; Zinc layered hydroxide; Intercalation
Depositing User: Mas Norain Hashim
Date Deposited: 10 Nov 2022 04:04
Last Modified: 10 Nov 2022 04:04
Altmetrics: http://www.altmetric.com/details.php?domain=psasir.upm.edu.my&doi=10.1080/14328917.2016.1265248
URI: http://psasir.upm.edu.my/id/eprint/62831
Statistic Details: View Download Statistic

Actions (login required)

View Item View Item