Citation
Rafiee-Moghaddam, Roshanak and Salimon, Jumat and Haron, Md. Jelas and Jahangirian, Hossein
(2013)
Jatropha curcas seed oil as new substrate for enzymatic methylhydroxylaminolysis.
Digest Journal of Nanomaterials and Biostructures, 8 (1).
pp. 415-422.
ISSN 1842-3582
Abstract
Synthesis of methyl fatty hydroxamic acids (MFHAs) was carried out using lipozyme RM
IM based on Jatropha Curcas seed oil. Optimized conditions were obtained at a mole ratio
of 6/1 of methyl hydroxylamine/oil, temperature at 41˚C, enzyme 30mg/mmol and 72 h of
reaction time. At this optimal condition, the yield% of methyl fatty hydroxamic based on
Jatropha Curcas seed oil was 93.92%. The product was characterized by Fourier
transform infrared (FTIR), and proton and carbon nuclear magnetic resonance (¹H-NMR
and ¹³C NMR) spectra.
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