Citation
Huang, Nay Ming and Lim, Hong Ngee and Radiman, Shahidan and Khiew, Poi Sim and Chiu, Wee Siong and Hashim, Rauzah and Chia, Chin Hua
(2010)
Sucrose ester micellar-mediated synthesis of Ag nanoparticles and the antibacterial properties.
Colloids and Surfaces A: Physicochemical and Engineering Aspects, 353 (1).
pp. 69-76.
ISSN 0927-7757; ESSN: 1873-4359
Abstract
Ag nanoparticles with diameter in the range of 10–25 nm had been synthesized using a simple sucrose ester micellar-mediated method. Ag nanoparticles were formed by adding AgNO3 solution into the sucrose ester micellar solution containing sodium hydroxide at atmospheric condition after 24 h of aging time. Trace amount of dimethyl formamide (DMF) in the sucrose ester solution served as a reducing agent while NaOH acted as a catalyst. The produced Ag nanoparticles were highly stable in the sucrose ester micellar system as there was no precipitation after 6 months of storage. The as-synthesized Ag nanoparticles were characterized using transmission electron microscope (TEM), X-ray diffractometer (XRD), dynamic light scattering (DLS) and UV–vis spectroscopy (UV–vis). Formation mechanism of Ag nanoparticles in the micellar-mediated synthesis is postulated. The antibacterial properties of the Ag nanoparticles were tested against Methicillin-resistant Staphylococcus aureus (MRSA) (Gram-positive) and Aeromonas hydrophila (Gram-negative) bacteria. This work provides a simple and “green” method for the synthesis of highly stable Ag nanoparticles in aqueous solution with promising antibacterial property.
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