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Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method.


Citation

Fard Masoumi, Hamid Reza and Kassim, Anuar and Basri, Mahiran and Abdullah, Dzulkefly Kuang (2011) Determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (TEA)-based esterquat cationic surfactant by a Taguchi Robust design method. Molecules, 16 (6). pp. 4672-4680. ISSN 1431-5157; ESSN:1420-3049

Abstract

A Taguchi robust design method with an L₉ orthogonal array was implemented to optimize experimental conditions for the biosynthesis of triethanolamine (TEA)-based esterquat cationic surfactants using an enzymatic reaction method. The esterification reaction conversion% was considered as the response. Enzyme amount, reaction time, reaction temperature and molar ratio of substrates, [oleic acid: triethanolamine (OA:TEA)] were chosen as main parameters. As a result of the Taguchi analysis in this study, the molar ratio of substrates was found to be the most influential parameter on the esterification reaction conversion%. The amount of enzyme in the reaction had also a significant effect on reaction conversion%.


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Additional Metadata

Item Type: Article
Divisions: Faculty of Science
DOI Number: https://doi.org/10.3390/molecules16064672
Publisher: MDPI
Keywords: Optimum conditions; Lipase-catalyzed synthesis; Triethanolamine (TEA)-Based Esterquat; Cationic surfactant; Taguchi Robust design method.
Depositing User: Nur Farahin Ramli
Date Deposited: 16 Aug 2013 03:44
Last Modified: 18 Sep 2015 08:19
Altmetrics: http://www.altmetric.com/details.php?domain=psasir.upm.edu.my&doi=10.3390/molecules16064672
URI: http://psasir.upm.edu.my/id/eprint/24951
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