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Response surface methodological (RSM) approach for optimizing the mechanical properties of starch-based films incorporated with chitosan-encapsulated thymol


Citation

Ahmad Shapi’i, Ruzanna and Othman, Siti Hajar and Naim, Mohd Nazli and Mohamed Amin Tawakkal, Intan Syafinaz and Mohd Basri, Mohd Salahuddin (2025) Response surface methodological (RSM) approach for optimizing the mechanical properties of starch-based films incorporated with chitosan-encapsulated thymol. Physica Scripta, 100 (9). art. no. 095012. pp. 1-12. ISSN 0031-8949; eISSN: 1402-4896

Abstract

In this study, starch-based films incorporated with glycerol and chitosan-encapsulated thymol (CNP-T) were formulated for potential active packaging applications. The central composite design (CCD) technique was used to formulate the films and 42 runs were generated based on three replications on two factors at five levels, particularly the concentration of glycerol (V1: 0, 6.25, 12.5, 18.75, 25% wt/wt of starch) and concentration of CNP-T (V2: 0, 0.2, 0.4, 0.6, 0.8% wt/v of starch). The optimized values for V1 and V2 were found to be 25% wt/wt and 0.8% wt/v, respectively, whereby the predicted values of the tensile strength (TS) and elongation at break (EAB) were 17.40 MPa and 40.01%, respectively. The optimized formulation offers a promising foundation for producing starch-based films containing CNP-T with enhanced mechanical properties, suitable for sustainable active packaging applications in the food industry.


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Additional Metadata

Item Type: Article
Subject: Atomic and Molecular Physics, and Optics
Subject: Mathematical Physics
Divisions: Faculty of Engineering
Institute of Nanoscience and Nanotechnology
DOI Number: https://doi.org/10.1088/1402-4896/ae02f8
Publisher: Institute of Physics
Keywords: Additives; Biomaterial; Blend; Casting; Film; Packaging
Depositing User: Ms. Nur Faseha Mohd Kadim
Date Deposited: 09 Mar 2026 07:01
Last Modified: 09 Mar 2026 07:01
Altmetrics: http://www.altmetric.com/details.php?domain=psasir.upm.edu.my&doi=10.1088/1402-4896/ae02f8
URI: http://psasir.upm.edu.my/id/eprint/123414
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