UPM Institutional Repository

Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions


Citation

Emmanuel Ibukun, Aduloju and Yahaya, Noorfatimah and Husaini Mohamed, Ahmad and Semail, Nadhiratul-Farihin and Abd Hamid, Muhammad Ariffuddin and Nadhirah Mohamad Zain, Nur and Anuar Kamaruddin, Mohammad and Hong Loh, Saw and Kamaruzaman, Sazlinda (2024) Recent developments in synthesis and characterisation of graphene oxide modified with deep eutectic solvents for dispersive and magnetic solid-phase extractions. Microchemical Journal, 199. art. no. 110111. pp. 1-16. ISSN 0026-265X; eISSN: 0026-265X

Abstract

Over the years, recent advancements have provided new insights into the functionalisation and synthesis of graphene oxide-based materials for sample preparation applications, utilising deep eutectic solvents (DESs). The demand for efficient, selective, innovative, and simple sample preparation of contaminants and pollutants from various matrices has rapidly focused on dispersive and magnetic solid-phase extraction. This study summarises the use of graphene oxide and reduced graphene materials in DES-based synthesis and functionalisation, along with their physicochemical characteristics and applications in dispersive and magnetic solid-phase extraction. The majority of DESs have demonstrated significant enhancements in the extraction of targeted analytes by increasing the effective surface area for active sites and introducing desired functionalities. Upon reviewing the existing literature, it was observed that DESs were functionalised either during or after the production of graphene materials. The findings highlight that dispersive and magnetic solid-phase extraction, incorporated with DES-functionalised graphene adsorbents, offer superior advantages for routine sample pretreatment of analytes, leading to enhanced analytical performance.


Download File

[img] Text
115320.pdf - Published Version
Restricted to Repository staff only

Download (3MB)

Additional Metadata

Item Type: Article
Divisions: Faculty of Science
DOI Number: https://doi.org/10.1016/j.microc.2024.110111
Publisher: Elsevier
Keywords: Deep eutectic solvent; Graphene oxide; Dispersive solid phase extraction; Magnetic solid phase extraction; Sample preparation
Depositing User: Ms. Che Wa Zakaria
Date Deposited: 10 Mar 2025 08:26
Last Modified: 10 Mar 2025 08:26
Altmetrics: http://www.altmetric.com/details.php?domain=psasir.upm.edu.my&doi=10.1016/j.microc.2024.110111
URI: http://psasir.upm.edu.my/id/eprint/115320
Statistic Details: View Download Statistic

Actions (login required)

View Item View Item