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Response surface optimization of multilayer graphene growth on alumina-supported bimetallic cobalt–nickel substrate


Alsaffar, May Ali and Abdul Rashid, Suraya and Ayodele, Bamidele Victor and Hamidon, Mohd Nizar and Md. Yasin, Faizah and Ismail, Ismayadi and Hosseini, Soraya and Babadi, Farahnaz Eghbali (2020) Response surface optimization of multilayer graphene growth on alumina-supported bimetallic cobalt–nickel substrate. Arabian Journal for Science and Engineering volume, 45. pp. 7455-7465. ISSN 2193-567X; ESSN: 2191-4281


This study investigates the optimization of multilayer graphene (MLG) growth on Co–Ni/Al2O3 substrate. The MLG synthesized by chemical vapor deposition technique (CVD) was characterized using various instrument techniques. The surface area and pore volume of the MLG were estimated as ~ 642 m2/g and ~ 2.7 cm3/g, respectively. The Raman spectrometric analysis showed evidence of MLG. The effects of parameters such as temperature, Co–Ni composition and ethanol flow rate were investigated using response surface methodology (RSM) and central composite design. The maximum MLG yield of 77% was attained at optimum conditions of 800 °C, Co–Ni composition of 0.3/0.7 and ethanol flow rate of 11 ml/min. The analysis of variance (ANOVA) results showed that the RSM quadratic model is significant with a p value < 0.0001. The coefficient of determination (R2) values of 0.9694 revealed the reliability of the RSM model. The potential of CVD as a technique to synthesize MLG growth of a highly ordered crystallinity structure has been demonstrated in this study. The resulting MLG films are promising materials for the use in improving graphene-based electronics, sensing and energy devices.

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Additional Metadata

Item Type: Article
Divisions: Faculty of Engineering
DOI Number: https://doi.org/10.1007/s13369-020-04586-4
Publisher: Springer
Keywords: Chemical vapor deposition; Characterization; Multilayer graphene; Response surface methodology; Optimization
Depositing User: Mohamad Jefri Mohamed Fauzi
Date Deposited: 30 May 2023 02:22
Last Modified: 30 May 2023 02:22
Altmetrics: http://www.altmetric.com/details.php?domain=psasir.upm.edu.my&doi=10.1007/s13369-020-04586-4
URI: http://psasir.upm.edu.my/id/eprint/87468
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