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A simple method for measuring intrinsic blocking temperature in superparamagnetic nanomaterials


Citation

Bahmanrokh, Ghazaleh and Hashim, Mansor and Ismail, Ismayadi and Soltani, Nayereh and Vaziri, Parisa and Shafie, Mohd Shamsul Ezzad and Navasery, Manizheh (2013) A simple method for measuring intrinsic blocking temperature in superparamagnetic nanomaterials. Journal of Superconductivity and Novel Magnetism, 26 (2). pp. 407-414. ISSN 1557-1939; ESSN: 1557-1947

Abstract

Temperature-dependent magnetic flux density (B) data, clearly exhibiting a transition temperature called intrinsic blocking temperature for some metallic samples in zero field cooled-warmed (ZFC-W) curves without employing an external magnetic field, has been obtained by a simple method. The reasons of the increase and decrease in the measured B-field at low temperature in zero magnetic-field were discussed. Co, CoPt3 and Co/Au, CoPt 3/Au core-shell nanoparticles, prepared by the reverse-micelle microemulsion method, were used as test materials. The blocking temperature was measured at a cusp of the measured magnetic field, B (produced by the sample), versus the temperature curve during warming up of the sample from a very low temperature (≤15 K) to room temperature. All the samples showed a blocking temperature at 45, 50, 40, and 42 K, respectively, for Co, CoPt3, Co/Au, and CoPt3/Au nanoparticles. A completely intrinsic behavior of the sample's magnetic moment was revealed by our method since no applied external field was used, yielding a truly spontaneous magnetization behavior.


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Additional Metadata

Item Type: Article
Divisions: Faculty of Science
Institute of Advanced Technology
DOI Number: https://doi.org/10.1007/s10948-012-1742-7
Publisher: Springer
Keywords: Anisotropy energy; Intrinsic blocking temperature; Magnetic flux density; Magnetic moment; Superparamagnetism; Zero field cooled-warmed
Depositing User: Nabilah Mustapa
Date Deposited: 05 Jun 2017 05:39
Last Modified: 05 Jun 2017 05:39
Altmetrics: http://www.altmetric.com/details.php?domain=psasir.upm.edu.my&doi=10.1007/s10948-012-1742-7
URI: http://psasir.upm.edu.my/id/eprint/52282
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