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Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations


Citation

Elsupikhe, Randa Fawzi and Shameli, Kamyar and Ahmad, Mansor B. (2015) Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations. Research on Chemical Intermediates, 41 (11). pp. 8515-8525. ISSN 0922-6168; ESSN: 1568-5675

Abstract

A green sonochemical method was developed for preparing silver nanoparticles (Ag-NPs) in j-carrageenan in different concentrations of AgNO3. The j-carrageenan was used as an eco-friendly stabilizer and ultrasonic irradiation as a green reducing agent. The number of Ag-NPs increased with increasing concentrations of AgNO3. Formation of Ag/j-carrageenan was determined by UV–visible spectroscopy where the surface plasmon absorption maximum was observed at 410–416 nm. XRD analysis showed the Ag-NPs are of a face-centered cubic structure. TEM images showed the well-dispersed Ag-NPs with an average particle size \5 nm. SEM images showed the spherical shape of the Ag-NPs. The FT-IR spectrum indicated the presence of j-carrageenan in capping the Ag-NPs. The use of photo irradiation provides a green and economic method features to the synthesis reported in this study.


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Additional Metadata

Item Type: Article
Divisions: Faculty of Science
DOI Number: https://doi.org/10.1007/s11164-014-1907-z
Publisher: Springer
Keywords: Green method; Ultrasonic irradiation; Silver nanoparticles; κ-carrageenan; Silver nitrate
Depositing User: Ms. Ainur Aqidah Hamzah
Date Deposited: 17 Jun 2022 08:23
Last Modified: 17 Jun 2022 08:23
Altmetrics: http://www.altmetric.com/details.php?domain=psasir.upm.edu.my&doi=10.1007/s11164-014-1907-z
URI: http://psasir.upm.edu.my/id/eprint/46343
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