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An optimization study for transesterification of palm oil using response surface methodology (RSM)


Citation

Wong, Yee Ching and Tan, Yen Ping and Yap, Taufiq Yun Hin and Ramli, Irmawati (2015) An optimization study for transesterification of palm oil using response surface methodology (RSM). Sains Malaysiana, 44 (2). pp. 281-290. ISSN 0026-6039

Abstract

Biodiesel was produced via transesterification of palm oil with methanol in the presence of CaO-Nb2 O5 mixed oxide catalyst. Response surface methodology (RSM) with central composite design (CCD) was performed to determine the optimum operating conditions and to optimize the biodiesel yield. In this study, the reaction variables being optimized were reaction time, catalyst loading and methanol to oil molar ratio. From the analysis of variance (ANOVA), the most influential parameter on biodiesel production was reaction time. The predicted yield was found in good agreement with the experimental value, with R2 = 0.9902. The optimum biodiesel yield of 97.67% was achieved at 2.67 h reaction time, with 3.60 wt. % of catalyst and with methanol to oil molar ratio of 13.04. The high biodiesel yield can be correlated to the synergic effect of basicity between the metallic ions of CaO-Nb2 O5 shown in the physicochemical analysis.


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Additional Metadata

Item Type: Article
Divisions: Faculty of Science
Publisher: Penerbit Universiti Kebangsaan Malaysia
Keywords: Biodiesel; Optimization; Palm oil; RSM; Transesterification
Depositing User: Mohd Hafiz Che Mahasan
Date Deposited: 20 Sep 2016 05:02
Last Modified: 15 May 2018 06:37
URI: http://psasir.upm.edu.my/id/eprint/43734
Statistic Details: View Download Statistic

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