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Synthesis of palm oil-based fatty methylhydrazide

Al-Mulla, Emad A. Jaffar and Ibrahim, Nor Azowa and Al-Karkhi, Isam Hussain T. and Shameli, Kamyar and Zidan, Mohammed and Ahmad, Mansor and Wan Yunus, Wan Md. Zin (2013) Synthesis of palm oil-based fatty methylhydrazide. Research on Chemical Intermediates, 39 (5). pp. 2133-2139. ISSN 0922-6168; ESSN: 1568-5675

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Official URL: http://dx.doi.org/10.1007/s11164-012-0745-0

Abstract

Fatty methylydrazides (FMHs) have been successfully synthesized from palm oil. Glycerol was produced as a by-product. The synthesis was carried out by reflux palm oil with methylhydrazine in hexane. FMHs have been characterized using elemental analysis, Fourier transform infrared spectroscopy and 1H nuclear magnetic resonance technique. The results showed that a 6:1 molar ratio of palm oil to methylhydrazine, a round 78 % maximum conversion of palm oil into FMHs and a 10 h reaction time are the optimum reaction conditions.

Item Type:Article
Keyword:Fatty methylhydrazide; Hexane; Palm oil
Faculty or Institute:Faculty of Science
Publisher:Springer Netherlands
DOI Number:10.1007/s11164-012-0745-0
ID Code:30010
Deposited By: Umikalthom Abdullah
Deposited On:30 May 2014 15:36
Last Modified:12 Feb 2016 15:21

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