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Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method


Citation

Tan, Yee Wean and Ramli, Irmawati and Yap, Taufiq Yun Hin (2007) Effect of calcination temperature on the characteristics of MoV oxides prepared via reflux method. The Malaysian Journal of Analytical Sciences, 11 (1). pp. 145-153. ISSN 1394-2506

Abstract / Synopsis

In this study, MoV mixed oxides with a molar ratio of 10:3 were prepared by reflux method. The samples were subjected to various calcination temperatures in order to investigate the physicochemical properties of the oxide affected by the parameter. Samples were characterised by XRD, TG/DTA, BET surface area, SEM and TPR. By imposing various calcination temperatures, phase evolutions were observed. However, these changes do not significantly affect the morphology, surface area, particle size and reducibility of the oxide. Still, the best calcination temperature can be chosen to arrive at the effective catalyst necessary for the desired catalytic reaction.


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Additional Metadata

Item Type: Article
Divisions: Faculty of Science
Publisher: Malaysian Analytical Sciences Society
Keywords: Mo-V-O catalysts; Reflux; Selective oxidation of propane; TPR
Depositing User: Najwani Amir Sariffudin
Date Deposited: 21 Apr 2011 16:14
Last Modified: 25 Nov 2016 17:13
URI: http://psasir.upm.edu.my/id/eprint/11938
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